《有机化学实验(一)》课程实验教学大纲
一、课程概况(Course Outline)
课程名称：有机化学实验(一)
Course: Experiments in Organic Chemistry Ⅰ
课程编号：0070300058适用学生：化学及应用化学专业
Course Number: 0070300058 Designed for: Chemistry and Applied Chemistry
学分： 2 学时：72 独立设课：是
Credit: 2 Workload: 72 Independent course: yes
预修课程：无机化学实验
Prior Learning: Experiments in Inorganic Chemistry
二、课程简介(Course Descriptions)
有机化学实验是一门独立的基础课程，由性质实验、基本操作实验、制备实验、设计性实验四部分组成。该课程目的在于训练学生基本操作技能，让学生掌握简单有机化合物的合成、纯化及结构测定方法；加深学生对化学基础理论、基本知识的理解，提高观察、分析和解决实际问题的能力，培养学生严谨的工作作风和实事求是的科学态度。
As an independent fundamental course, Experiments in Organic Chemistry includes four sections, identification of organic compounds, acquisition of basic laboratory skill, preparation of organic compounds, and design of organic experiments. Students are supposed to acquire the basic experiment skills and knowledge for preparation, purification, and identification of regular organic compounds. The course gives students a deeper understanding of fundamental experimental organic chemistry and exposes students to each technique in a systematic and in-depth way. Also, it trains students with the problem-solving ability as well as with strictness and scientific attitude.
三、实验项目一览表(Experiment List)
序号 No. | 实验名称 Title | 每组人数 Number of Students in each group | 实验 时数 Hours | 实验类型 验证∕综合∕设计 Experimental Type Characterization/Comprehensiveness /Designment | 必做∕选做 Compulsory /Optional |
1 | 仪器及实验室安全知识介绍 Introduction of Instruments and Safty Rules in Organic Chemistry Laboratory | 1 | 4 | 验证 Characterization | 必做 Compulsory |
2 | 熔点测定 Determination of Melting Point | 1 | 4 | 验证 Characterization | 必做 Compulsory |
3 | 蒸馏、沸点测定 Distillation and Determination of Boiling Point | 1 | 4 | 验证 Characterization | 必做 Compulsory |
4 | 重结晶 Recrystallization | 1 | 4 | 验证 Characterization | 必做 Compulsory |
5 | 水蒸气蒸馏 Steam Distillation | 1 | 4 | 验证 Characterization | 必做 Compulsory |
6 | 折光率的测定 Determination of Refractive Index | 1 | 4 | 验证 Characterization | 选做 Optional |
7 | 无水乙醇的制备 Preparation of Anhydrous Ethanol | 1 | 4 | 验证 Characterization | 必做 Compulsory |
8 | 薄层色谱 Thin-Layer Chromatography | 1 | 4 | 验证 Characterization | 必做 Compulsory |
9 | 不饱和烃的制备及其性质 Preparation and Properties of Unsaturated Hydrocarbons | 1 | 4 | 验证 Characterization | 选做 Optional |
10 | 苯乙酮的制备 Preparation of Acetophenone | 1 | 4 | 验证 Characterization | 选做 Optional |
11 | 反-1,2-二氨基环己烷的手性拆分及其旋光度的测定 Separation and Determination of trans-1,2-diamino cyclohexane | 1 | 8 | 综合 Comprehensiveness | 必做 Compulsory |
12 | 1-溴丁烷的制备 Preparation of 1-Bromobutane | 1 | 8 | 验证 Characterization | 必做 Compulsory |
13 | 正丁醚的制备 Preparation of Dibutyl Ether | 1 | 4 | 验证 Characterization | 必做 Compulsory |
14 | 2-甲基-2-丁醇的制备 Preparation of 2-Methylbutan-2-ol | 1 | 8 | 验证 Characterization | 必做 Compulsory |
15 | 二苯甲醇的氧化 Oxidation of Diphenylmethanol | 1 | 4 | 验证 Characterization | 必做 Compulsory |
16 | 文献实验(1, 1′-联二萘酚的合成) Preparation of 2,2'-Dihydroxy-1,1'-binaphthyl | 1 | 4 | 设计 Designment | 选做 Optional |
四、推荐教材及参考书目(Recommended Reading)
1.推荐教材
有机化学实验，曾绍琼主编，高等教育出版社，2000年，第三版。
Recommended Teaching Materials:
Experiments in Organic Chemistry，Shaoqiong Zeng, Higher Education Press, 2000, 3rd edition.
2.参考书目
有机化学实验, 兰州大学、复旦大学化学系有机化学教研室编，高等教育出版社，2002年，第二版。
Reference Books:
Experiments in Organic Chemistry，Chemical Department of Fudan University and Lanzhou University, Higher Education Press, 2002, 2ndedition.
五、考核与评价方式(Course Evaluation)
考核与评价方式：结合实验预习、实验操作、实验结果、实验报告、纪律卫生等情况给出平时成绩；平时成绩占总成绩的70%, 期末操作考核占总成绩的30%。
The assessment consists of laboratorial preview, laboratorial skill, experimental results, the final written report, and the conduct of the duty on sanitation etc, which in total counts for the score for practical. The final score is derived from practical (70%) and final exam (30%).
《有机化学实验(二)》课程实验教学大纲
一、课程概况(Course Outline)
课程名称：有机化学实验(二)
Course： Experiments in Organic Chemistry Ⅱ
课程编号： 0070300059 适用学生：化学及应用化学专业
Course Number: 0070300059 Designed for: Chemistry and Applied Chemistry
学分：2 学时：64 独立设课：是
Credit: 2 Workload: 64 Independent Course: yes
预修课程：无机化学实验
Prior Learning: Experiments in Inorganic Chemistry
二、课程简介(Course Descriptions)
有机化学实验是一门独立的基础课程，由性质实验、基本操作实验、制备实验、设计性实验四部分组成。该课程目的在于训练学生基本操作技能，让学生掌握简单有机化合物的合成、纯化及结构测定方法；加深学生对化学基础理论、基本知识的理解，提高观察、分析和解决实际问题的能力，培养学生严谨的工作作风和实事求是的科学态度。
As an independent fundamental course, Experiments in Organic Chemistry includes four sections, identification of organic compounds, acquisition of basic laboratory skill, preparation of organic compounds, and design of organic experiments. Students are supposed to acquire the basic experiment skills and knowledge for preparation, purification, and identification of regular organic compounds. The course gives students a deeper understanding of fundamental experimental organic chemistry and exposes students to each technique in a systematic and in-depth way. Also, it trains students with the problem-solving ability as well as with strictness and scientific attitude.
三、实验项目一览表(Experiment project schedule)
序号 No. | 实验名称 Title | 每组人数 Number of Students in each group | 实验 时数 Hours | 实验类型 验证∕综合∕设计 Experimental Type Characterization/Comprehensiveness /Designment | 必做∕选做 Compulsory /Optional |
1 | 二苄叉丙酮的制备 Preparation of 1,5-diphenylpenta-1,4-dien-3-one | 1 | 4 | 验证 Characterization | 必做 Compulsory |
2 | 乙酰苯胺的制备 Preparation of N-phenylacetamide | 1 | 4 | 验证 Characterization | 必做 Compulsory |
3 | 肉桂酸的制备 Preparation of Cinnamic Acid | 1 | 8 | 验证 Characterization | 必做 Compulsory |
4 | 安息香缩合反应 Benzoin Condensation | 1 | 4 | 验证 Characterization | 选做 Optional |
5 | 甲基橙制备 Preparation of Methyl Orange | 1 | 4 | 验证 Characterization | 选做 Optional |
6 | 二苯甲醇的制备 Preparation of Diphenylmethanol | 1 | 4 | 验证 Characterization | 必做 Compulsory |
7 | 乙酰乙酸乙酯制备 Preparation of Ethyl 3-oxobutanoate | 1 | 6 | 验证 Characterization | 必做 Compulsory |
8 | 呋喃甲醇和呋喃甲酸的制备 Preparation of Furan-2-carboxylic acid and Furan-2-ylmethanol | 1 | 6 | 验证 Characterization | 必做 Compulsory |
9 | 纸色谱 Paper Chromatography | 1 | 4 | 验证 Characterization | 必做 Compulsory |
10 | 生物碱的提取 Extraction of Alkaloids | 1 | 4 | 验证 Characterization | 必做 Compulsory |
11 | Dieles-Alder反应 Dieles-Alder Reaction | 1 | 4 | 验证 Characterization | 必做 Compulsory |
12 | 乙酸丁酯的制备及其含量测定 Preparation and Determination of Butyl acetate | 1 | 8 | 综合 Comprehensiveness | 必做 Compulsory |
13 | 乙酰水杨酸的制备 Preparation of 2-Acetoxybenzoic acid | 1 | 4 | 验证 Characterization | 选做 Optional |
14 | 2,3;5,6-二-O-异丙叉基-α-D-呋喃甘露糖的制备 Synthesis of 2,3;5,6-di-Oisopropylidene-a-D-gulofuranose | 1 | 4 | 设计 Designment | 必做 Compulsory |
四、推荐教材及参考书目(Recommended Reading)
1.推荐教材
有机化学实验，曾绍琼主编，高等教育出版社，2000年，第三版。
Recommended Teaching Materials:
Experiments in Organic Chemistry，Shaoqiong Zeng, Higher Education Press, 2000, 3rd edition.
2.参考书目
有机化学实验, 兰州大学、复旦大学化学系有机化学教研室编，高等教育出版社，2002年，第二版。
Reference Books:
Experiments in Organic Chemistry，Chemical Department of Fudan University and Lanzhou University, Higher Education Press, 2002, 2ndedition.
五、考核与评价方式(Course Evaluation)
考核与评价方式：结合实验预习、实验操作、实验结果、实验报告、纪律卫生等情况给出平时成绩；平时成绩占总成绩的70%, 期末操作考核占总成绩的30%。
The assessment consists of laboratorial preview, laboratorial skill, experimental results, the final written report, and the conduct of the duty on sanitation etc, whi, ch in total counts for the score for practical. The final score is derived from practical (70%) and final exam (30%).